2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate

Base Information

Chemical Name:2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate
CAS No.:1159415-87-8
Molecular Formula:CF₃O₃S*C₄₂H₃₃N₂P₂
Molecular Weight:776.755
Hs Code.:

Synonyms:2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate

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Chemical Property of 2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate

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Technology Process of 2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate

There total 1 articles about 2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1159415-85-6
2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-1H-benzimidazole

: 333-27-7
methyl trifluoromethanesulfonate

: 1159415-87-8
2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/ejic.200800157

Reference yield: 97.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 1159415-87-8
2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium trifluoromethanesulfonate

: 1159415-91-4
[[2-(diphenylphosphanyl)-N-(2'-diphenylphosphanyl-1'-naphthyl)-N'-methyl-1H-benzimidazolium]palladium(II) dichloride] trifluoromethanesulfonate

Guidance literature:: In tetrahydrofuran; (Ar), stoich., Pd complex and ligand dissolved in THF at -20°C, stirred for 2 h; concd.(vac.), washed (Et2O), recrystd. at -20°C (CH2Cl/pentane), elem. anal.;
DOI:10.1002/ejic.200800157