Ni₂(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid^(1-))2(2,2'-bipyridine)2

Base Information

• Chemical Name: Ni₂(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid^(1-))2(2,2'-bipyridine)2
• CAS No.: 869707-54-0
• Molecular Formula: C₄₄H₃₀N₄Ni₂O₁₂
• Molecular Weight: 924.122

Synonyms:Ni₂(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid^(1-))2(2,2'-bipyridine)2

Chemical Property of Ni₂(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid^(1-))2(2,2'-bipyridine)2

Chemical Property:

Purity/Quality:

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Technology Process of Ni₂(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid^(1-))2(2,2'-bipyridine)2

There total 1 articles about Ni₂(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid^(1-))2(2,2'-bipyridine)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

[2,2]bipyridinyl (366-18-7) + nickel(II) chloride hexahydrate + terephthalic acid (100-21-0) → Ni2(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid(1-))2(2,2'-bipyridine)2 (869707-54-0)

Guidance literature:

With KOH; In water; High Pressure; mixt. NiCl2*6H2O, 1,4-benzenedicarboxylic acid, KOH, 2,2'-bipyridine (1:1:2:1) and water in stainless steel reactor with Teflon liner was heatedat 150°C for 48 h; crystals were filtered and washed with water and acetone; elem. anal.;

DOI:10.1021/ic050644d

Reference yield:

Ni2(1,4-benzenedicarboxylate)(1,4-benzenedicarboxylic acid(1-))2(2,2'-bipyridine)2 (869707-54-0) → nickel(II) oxide (1313-99-1)

Guidance literature:

In neat (no solvent, solid phase); heating to 600°C; X-ray powder diffraction;

DOI:10.1021/ic050644d

upstream raw materials:

[2,2]bipyridinyl

terephthalic acid

Downstream raw materials:

nickel(II) oxide

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