C₅₀H₄₆O₁₅S

Base Information

Chemical Name:C₅₀H₄₆O₁₅S
CAS No.:874479-75-1
Molecular Formula:C₅₀H₄₆O₁₅S
Molecular Weight:918.972
Hs Code.:

C<sub>50</sub>H<sub>46</sub>O<sub>15</sub>S

Synonyms:C₅₀H₄₆O₁₅S

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Chemical Property of C₅₀H₄₆O₁₅S

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Technology Process of C₅₀H₄₆O₁₅S

There total 9 articles about C₅₀H₄₆O₁₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874479-74-0
methyl 4,6-O-benzylidene-3-O-(chloroacetyl)-β-D-galactopyranosyl-(1->4)-O-β-D-glucopyranoside

: 874479-75-1
C₅₀H₄₆O₁₅S

Guidance literature:: Multi-step reaction with 6 steps

1: 50 percent / molecular sieves 4 Angstroem; DMAP; pyridine / CH₂Cl₂ / 0 - 20 °C

2: 78 percent / hydrazinium acetate / dimethylformamide / 20 - 40 °C

3: pyridine / CH₂Cl₂ / -78 - 0 °C

4: 426 mg / KNO₂ / dimethylformamide / 20 - 50 °C

5: pyridine / CH₂Cl₂ / -78 - 20 °C

6: 613 mg / dimethylformamide / 20 - 50 °C

With pyridine; dmap; potassium nitrite; 4 A molecular sieve; hydrazinium monoacetate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.08.057

Reference yield:

: 98-88-4
benzoyl chloride

: 874479-75-1
C₅₀H₄₆O₁₅S

Guidance literature:: Multi-step reaction with 6 steps

1: 50 percent / molecular sieves 4 Angstroem; DMAP; pyridine / CH₂Cl₂ / 0 - 20 °C

2: 78 percent / hydrazinium acetate / dimethylformamide / 20 - 40 °C

3: pyridine / CH₂Cl₂ / -78 - 0 °C

4: 426 mg / KNO₂ / dimethylformamide / 20 - 50 °C

5: pyridine / CH₂Cl₂ / -78 - 20 °C

6: 613 mg / dimethylformamide / 20 - 50 °C

With pyridine; dmap; potassium nitrite; 4 A molecular sieve; hydrazinium monoacetate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.08.057

Reference yield:

: 137119-40-5
methyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

: 874479-75-1
C₅₀H₄₆O₁₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: Bu₂SnO / methanol / 2 h / Heating

1.2: 70 percent / molecular sieves 4 Angstroem / toluene / 0.5 h / 0 °C

2.1: 50 percent / molecular sieves 4 Angstroem; DMAP; pyridine / CH₂Cl₂ / 0 - 20 °C

3.1: 78 percent / hydrazinium acetate / dimethylformamide / 20 - 40 °C

4.1: pyridine / CH₂Cl₂ / -78 - 0 °C

5.1: 426 mg / KNO₂ / dimethylformamide / 20 - 50 °C

6.1: pyridine / CH₂Cl₂ / -78 - 20 °C

7.1: 613 mg / dimethylformamide / 20 - 50 °C

With pyridine; dmap; potassium nitrite; 4 A molecular sieve; hydrazinium monoacetate; di(n-butyl)tin oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.08.057