benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate

Base Information

Chemical Name:benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate
CAS No.:1005348-23-1
Molecular Formula:C₂₀H₂₀IN₃O₄
Molecular Weight:493.301
Hs Code.:

Synonyms:benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate

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Chemical Property of benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate

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Technology Process of benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate

There total 2 articles about benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 955030-16-7,957774-11-7
N-allyl-N',N-bis-Cbz-guanidine

: 1005348-23-1
benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate

Guidance literature:: With iodine; potassium carbonate; In acetonitrile; at -15 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2014.03.087

Reference yield:

: 152120-55-3
N,N-bis(benzyloxycarbonyl)-1H-pyrazole-1-carboxamidine

: 1005348-23-1
benzyl 1-((benzyloxy)carbonyl)-5-(iodomethyl)imidazolidin-2-ylidenecarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 16 h / 20 °C / Inert atmosphere

2: iodine; potassium carbonate / acetonitrile / 16 h / -15 - 20 °C / Inert atmosphere

With iodine; potassium carbonate; In acetonitrile;
DOI:10.1016/j.tet.2014.03.087