N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

Base Information

• Chemical Name: N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine
• CAS No.: 1616724-78-7
• Molecular Formula: C₃₁H₄₃N₃O₆
• Molecular Weight: 553.699

Synonyms:N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

Chemical Property of N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

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Technology Process of N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

There total 1 articles about N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N1-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine (1126795-15-0) + Ethyl oxalyl chloride (4755-77-5) → N1-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine (1616724-78-7)

Guidance literature:

In dichloromethane; at 0.25 ℃; for 2h;

Reference yield:

N1-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine (1616724-78-7) → 2-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-yl(2-(carboxyformamido)phenyl)amino)-2-oxoacetic acid (1616724-07-2)

Guidance literature:

N₁-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyco[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine; With water; sodium hydroxide; In ethanol; at 0.25 ℃; for 1h;

With hydrogenchloride; In water; pH=4;

upstream raw materials:

N₁-((1R,1'R,3R,3'R,5S,5'S)-[3,9'-bi(9'-azabicyclo[3.3.1]nonan)]-3'-yl)benzene-1,2-diamine

Ethyl oxalyl chloride

Downstream raw materials:

2-((1R,1'R,3r,3'R,5S,5'S,9's)-[3,9'-bi(bicyclo[3.3.1]nonan)]-3'-yl(2-(carboxyformamido)phenyl)amino)-2-oxoacetic acid

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