N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide

Base Information

Chemical Name:N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide
CAS No.:1292810-20-8
Molecular Formula:C₁₉H₁₇Cl₂N₃O₆S
Molecular Weight:486.332
Hs Code.:

Synonyms:N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide

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Technology Process of N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide

There total 2 articles about N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1292810-04-8
N-((1R,2R)-2-(2,6-dichlorophenylthio)cyclohexyl)-3,5-dinitrobenzamide

: 1292810-20-8
N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c0cc05840h

Reference yield:

: 884588-09-4
7-(3,5-dinitrobenzoyl)-7-azabicyclo[4.1.0]heptane

: 24966-39-0
2,6-dichlorothiophenol

: 1292810-20-8
N-((1R,2R)-2-(2,6-dichlorophenylsulfinyl)cyclohexyl)-3,5-dinitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1R,2R)-2-(tert-butyldiphenylsilyloxy)-N-(dipyrrolidin-1-ylmethylene)-2,3-dihydro-1H-inden-1-amine / diethyl ether / 0.5 h / -50 °C / Inert atmosphere

1.2: -50 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

With (1R,2R)-2-(tert-butyldiphenylsilyloxy)-N-(dipyrrolidin-1-ylmethylene)-2,3-dihydro-1H-inden-1-amine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1039/c0cc05840h