allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane

Base Information

• Chemical Name: allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane
• CAS No.: 1227937-57-6
• Molecular Formula: C₂₆H₂₁F₁₇Si
• Molecular Weight: 684.511

Synonyms:allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane

Chemical Property of allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane

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Technology Process of allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane

There total 1 articles about allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

allylchloro(methyl)phenylsilane (112945-35-4) + 1-(4'-bromophenyl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane (195324-88-0) → allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane (1227937-57-6)

Guidance literature:

1-(4'-bromophenyl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -30 ℃; Inert atmosphere;

allylchloro(methyl)phenylsilane; In tetrahydrofuran; diethyl ether; hexane; at -30 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.jfluchem.2009.05.017

Reference yield: 36.0%

allyl(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)phenyl)(methyl)(phenyl)silane (1227937-57-6) + 1-cyclohexenyl methyl ketone (932-66-1) → 1-acetyl-8-((4-(3',3',4',4',5',5',6',6',7',7',8',8',9',9',10',10',10'-heptadecafluorodecyl)phenyl)methylphenylsilyl)bicyclo[4.3.0]nonane

Guidance literature:

With titanium tetrachloride; In dichloromethane; at -78 - -20 ℃; Inert atmosphere;

DOI:10.1016/j.jfluchem.2009.05.017

upstream raw materials:

allylchloro(methyl)phenylsilane

1-(4'-bromophenyl)-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecane

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