7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

Base Information

Chemical Name:7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide
CAS No.:130220-21-2
Molecular Formula:C₂₅H₃₈O₂S₃Si
Molecular Weight:494.859
Hs Code.:

Synonyms:7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

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Chemical Property of 7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

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Technology Process of 7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

There total 7 articles about 7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 5799-67-7
dimethyl(methylthio)sulfonium tetrafluoroborate

: 130220-22-3
3-(trimethylsilyl)-1-phenyl-3-(phenylsulfonyl)-9-<<2-(trimethylsilyl)ethyl>thio>nonane

: 130220-21-2
7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

Guidance literature:: With Dimethyldisulphide; In dichloromethane; for 12h;

Reference yield:

: 17494-61-0
((3-phenylpropyl)sulfonyl)benzene

: 130220-21-2
7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to 25 deg C

2: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, -78 deg C, 15 min, 2.) from -78 deg C to RT, 4 h

3: 87 percent / sodium hydride / tetrahydrofuran / 1.) 0 deg C, 2.) RT, 5 min

4: 74 percent / methyl disulfide / CH₂Cl₂ / 12 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; Dimethyldisulphide; sodium hydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 130220-21-2
7-(trimethylsilyl)-9-phenyl-7-(phenylsulfonyl)nonanyl methyl disulfide

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / tetrahydrofuran / 1 h / 25 °C

2: 80percent m-chloroperbenzoic acid / CH₂Cl₂ / 25 °C

3: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to 25 deg C

4: 1.) hexamethylphosphoric triamide (HMPA), n-BuLi / 1.) THF, -78 deg C, 15 min, 2.) from -78 deg C to RT, 4 h

5: 87 percent / sodium hydride / tetrahydrofuran / 1.) 0 deg C, 2.) RT, 5 min

6: 74 percent / methyl disulfide / CH₂Cl₂ / 12 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; Dimethyldisulphide; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;