N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide
• CAS No.: 1379536-71-6
• Molecular Formula: C₃₄H₂₈FN₃O₂S
• Molecular Weight: 561.68

Synonyms:N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

Chemical Property of N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide

There total 1 articles about N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

N-2-butenyl-N-phenylethynyl-p-toluenesulfonamide + C22H17FN2O2S (1201945-53-0) → N-(but-3-en-2-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide (1379536-71-6) + (E)-N-(but-2-en-1-yl)-N-(8-fluoro-1,5-diphenylpyrazolo[5,1-a]isoquinolin-2-yl)-4-methylbenzenesulfonamide (1379536-75-0)

Guidance literature:

C₂₂H₁₇FN₂O₂S; With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 70 ℃; for 3h; Inert atmosphere;

N-2-butenyl-N-phenylethynyl-p-toluenesulfonamide; With palladium diacetate; caesium carbonate; triphenylphosphine; In 1,2-dichloro-ethane; toluene; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol301023m

upstream raw materials:

C₂₂H₁₇FN₂O₂S

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