salicylic acid (methylsulfonyl)methyl ester

Base Information

Chemical Name:salicylic acid (methylsulfonyl)methyl ester
CAS No.:76432-34-3
Molecular Formula:C₉H₁₀O₅S
Molecular Weight:230.241
Hs Code.:

Synonyms:salicylic acid (methylsulfonyl)methyl ester

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Chemical Property of salicylic acid (methylsulfonyl)methyl ester

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Technology Process of salicylic acid (methylsulfonyl)methyl ester

There total 4 articles about salicylic acid (methylsulfonyl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76432-29-6
methylthiomethyl 2-hydroxybenzoate

: 76432-34-3
salicylic acid (methylsulfonyl)methyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; Ambient temperature;
DOI:10.1002/jps.2600700708

Reference yield:

: 76432-35-4
methylsulfonylmethyl 2-acetoxybenzoate

: 76432-34-3
salicylic acid (methylsulfonyl)methyl ester

: 50-78-2,98201-60-6
aspirin

Guidance literature:: With 10 percent human plasma; In acetonitrile; at 37 ℃; Rate constant; phosphate buffer (pH 7.4); or in undiluted plasma;
DOI:10.1021/jm00123a040

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 76432-34-3
salicylic acid (methylsulfonyl)methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Et₃N / acetonitrile / 24 h / Heating

2: 85 percent / m-chloroperbenzoic acid / CHCl₃ / Ambient temperature

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; acetonitrile;
DOI:10.1002/jps.2600700708