methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

Base Information

Chemical Name:methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate
CAS No.:1345893-36-8
Molecular Formula:C₂₁H₂₂NO₃P
Molecular Weight:367.384
Hs Code.:

Synonyms:methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

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Chemical Property of methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

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Technology Process of methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

There total 3 articles about methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: methyl (Z)-3-acetamido-4-(diphenylphosphoryl)methylpent-2-enoate

: 1345893-36-8
methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/acs.joc.5b02347

Reference yield: 80.0%

: 3952-66-7
methyl 2-oxobutanoate

: 274677-02-0
2-diphenylphosphinoyl-3-ethyl-2H-azirine

: 1345893-36-8
methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

: methyl (Z)-3-acetamido-4-(diphenylphosphoryl)methylpent-2-enoate

Guidance literature:: methyl 2-oxobutanoate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

2-diphenylphosphinoyl-3-ethyl-2H-azirine; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.5b02347

Reference yield: 75.0%

: C₁₇H₁₇OP

: 105-45-3
acetoacetic acid methyl ester

: 1345893-36-8
methyl 5-(diphenylphosphoryl)-4-ethyl-2-methyl-1H-pyrrole-3-carboxylate

Guidance literature:: acetoacetic acid methyl ester; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

C₁₇H₁₇OP; In tetrahydrofuran; Inert atmosphere; Reflux;
DOI:10.1021/jo201932m