NbCl₃(HB(C₃N₂(CH₃)2Cl)3)

Base Information

Chemical Name:NbCl₃(HB(C₃N₂(CH₃)2Cl)3)
CAS No.:863609-49-8
Molecular Formula:C₁₅H₁₉BCl₆N₆Nb
Molecular Weight:599.791
Hs Code.:

NbCl<sub>3</sub>(HB(C<sub>3</sub>N<sub>2</sub>(CH<sub>3</sub>)2Cl)3)

Synonyms:NbCl₃(HB(C₃N₂(CH₃)2Cl)3)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of NbCl₃(HB(C₃N₂(CH₃)2Cl)3)

Chemical Property:

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Technology Process of NbCl₃(HB(C₃N₂(CH₃)2Cl)3)

There total 1 articles about NbCl₃(HB(C₃N₂(CH₃)2Cl)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 22943-66-4,38780-86-8,61247-57-2
tetrachlorobis(tetrahydrofuran)niobium(IV)

: 863609-60-3
Sn((CH₂)3CH₃)2Cl(HB(C₃N₂(CH₃)2Cl)3)

: 863609-49-8
NbCl₃(HB(C₃N₂(CH₃)2Cl)3)

: 683-18-1
dibutyltin chloride

Guidance literature:: In toluene; (N2); addn. of a soln. of tin complex in toluene to a suspn. of niobium complex in toluene at room temp., stirring for 4 d in the dark; evapn., addn. of CH2Cl2, stirring for 2 d, filtration, concn., addn. of hexane, crystn. at -25°C, washing with Et2O, drying in vac.; elem. anal.;
DOI:10.1021/om050423f

Reference yield:

: 863609-49-8
NbCl₃(HB(C₃N₂(CH₃)2Cl)3)

: 536-74-3
phenylacetylene

: 863609-52-3
NbCl₂(C₆H₅CCH)(HB(C₃N₂(CH₃)2Cl)3)

Guidance literature:: With Zn; In tetrahydrofuran; (N2); addn. of alkyne to a suspn. of niobium complex in THF with granular Zn at room temp., stirring overnight; evapn., addn. of toluene, evapn. twice, extn. with CH2Cl2 or toluene, addn. of pentane or hexane, filtration through Celite, repeated extn., evapn., recrystn. (CH2Cl2/pentane); elem. anal.;
DOI:10.1021/om050423f