diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate

Base Information

Chemical Name:diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate
CAS No.:1188429-26-6
Molecular Formula:C₂₇H₃₉N₃O₈
Molecular Weight:533.622
Hs Code.:

Synonyms:diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate

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Chemical Property of diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate

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Technology Process of diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate

There total 1 articles about diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1188429-25-5
benzyl cyano((1R,3S)-3-(hydroxymethyl)-1,2,2-trimethylcyclopentyl)methylcarbamate

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 1188429-26-6
diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate

Guidance literature:: benzyl cyano((1R,3S)-3-(hydroxymethyl)-1,2,2-trimethylcyclopentyl)methylcarbamate; With hydroxylamine; In ethanol; water; at 50 ℃; for 40h;

acetylenedicarboxylic acid diethyl ester; In ethanol; at 40 ℃; for 4h;

Reference yield: 27.0%

: 1188429-26-6
diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate

: 124-63-0
methanesulfonyl chloride

: ethyl (7S,10R)-11-(((benzyloxy)carbonyl)amino)-3-hydroxy-10,12,12-trimethyl-4-oxo-6,7,8,9,10,11-hexahydro-4H-7,10-methanopyrimido[1,2-a]azocine-2-carboxylate

Guidance literature:: diethyl 2-(1-amino-2-(benzyloxycarbonylamino)-2-((1R,3S)-3-(hydroxymethyl)-, 2,2-trimethylcyclopentyl)ethylideneaminooxy)but-2-enedioate; In xylene; at 125 - 130 ℃; for 8h;

methanesulfonyl chloride; With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 90 ℃; for 30h;