2,4,6-tribromophenyl 4-methylbenzenesulfonate

Base Information

Chemical Name:2,4,6-tribromophenyl 4-methylbenzenesulfonate
CAS No.:2437-48-1
Molecular Formula:C13H9 Br3 O3 S
Molecular Weight:484.9858
Hs Code.:
Mol file:2437-48-1.mol

Synonyms:Phenol,2,4,6-tribromo-, 4-methylbenzenesulfonate (9CI); Phenol, 2,4,6-tribromo-,p-toluenesulfonate (6CI); 2,4,6-Tribromophenyl 4-methylbenzenesulfonate;2,4,6-Tribromophenyl p-toluenesulfonate; NSC 2217

Suppliers and Price of 2,4,6-tribromophenyl 4-methylbenzenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of 2,4,6-tribromophenyl 4-methylbenzenesulfonate

Chemical Property:

Vapor Pressure:7.32E-10mmHg at 25°C
Boiling Point:505.9°C at 760 mmHg
Flash Point:259.8°C
Density:1.956g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4,6-tribromophenyl 4-methylbenzenesulfonate

There total 1 articles about 2,4,6-tribromophenyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 118-79-6
2,4,6-tribromophenol

: 2437-48-1
2,4,6-tribromophenyl 4-methylbenzenesulfonate

Guidance literature:: With N,N-diethylaniline;

Reference yield: 75.0%

: 2437-48-1
2,4,6-tribromophenyl 4-methylbenzenesulfonate

: 17435-72-2
ethyl 2-bromomethyl-2-propenoate

: 1187442-44-9
ethyl 2-(3,5-dibromo-2-{[(4-methylphenyl)sulfonyl]oxy}benzyl)acrylate

Guidance literature:: 2,4,6-tribromophenyl 4-methylbenzenesulfonate; With magnesium; lithium chloride; zinc; In tetrahydrofuran; at 25 ℃; for 1h; Inert atmosphere;

ethyl 2-bromomethyl-2-propenoate; With CCl₂CuN^(2-)*2Li⁽¹⁺⁾; In tetrahydrofuran; at -20 - 25 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900575

Reference yield: 74.0%

: 2437-48-1
2,4,6-tribromophenyl 4-methylbenzenesulfonate

: 1638-63-7
2-acetoxy-2-phenylacetyl chloride

: 1187442-43-8
2-(3,5-dibromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate

Guidance literature:: 2,4,6-tribromophenyl 4-methylbenzenesulfonate; With lithium chloride; zinc; In tetrahydrofuran; at 25 ℃; for 1h; Inert atmosphere;

With CCl₂CuN^(2-)*2Li⁽¹⁺⁾; In tetrahydrofuran; at -20 ℃; for 0.25h; Inert atmosphere;

2-acetoxy-2-phenylacetyl chloride; In tetrahydrofuran; at -20 - 25 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900575