Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane

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Chemical Name:Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane
CAS No.:115029-80-6
Molecular Formula:C₁₈H₂₄O₃Si
Molecular Weight:316.472
Hs Code.:

Synonyms:Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane

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Chemical Property of Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane

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Technology Process of Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane

There total 10 articles about Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 115029-78-2
1-(4,6-O-benzylidene-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-3,3-dimethyl-3-sila-1-butyne

: 115029-80-6
1-(4,6-O-benzylidene-2,3-dideoxy-α-D-erythro-hexopyranosyl)-3,3-dimethyl-3-sila-1-butene

Guidance literature:: With potassium diazodicarboxylate; acetic acid; In methanol; for 4.5h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90886-3

Reference yield:

: 81353-38-0
(trimethylsilylethynyl)tributyltin

: 115029-80-6
Trimethyl-[(Z)-2-((2R,4aR,6S,8aS)-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-6-yl)-vinyl]-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / TiCl₄ / 1 h

2: N₂H₂

With diazene; titanium tetrachloride;
DOI:10.1016/S0040-4039(00)74776-9

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 115029-80-6
1-(4,6-O-benzylidene-2,3-dideoxy-α-D-erythro-hexopyranosyl)-3,3-dimethyl-3-sila-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / camphorsulfonic acid / dimethylformamide / 6 h / 100 °C

2: 50 percent / dipotassium azodicarboxylate, acetic acid / methanol / 4.5 h / Ambient temperature

With camphor-10-sulfonic acid; potassium diazodicarboxylate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90886-3