N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine

Base Information

Chemical Name:N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine
CAS No.:76227-21-9
Molecular Formula:C₁₇H₂₁N₅O₅
Molecular Weight:375.384
Hs Code.:

Synonyms:N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine

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Chemical Property of N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine

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Technology Process of N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine

There total 6 articles about N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76227-20-8
1-benzyloxy-2'-deoxyadenosine perchlorate

: 76227-21-9
N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamido-1H-imidazole-4-carboxamidine

Guidance literature:: With Amberlite IRA-402 (HClO₃^-); In water;
DOI:10.1248/cpb.37.2601

Reference yield: 70.0%

: 76227-20-8
1-benzyloxy-2'-deoxyadenosine perchlorate

: 76227-21-9
N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamidoimidazole-4-carboxamidine

Guidance literature:: With Amberlite IRA-402 (HCO₃^-); water; at 3 - 4 ℃; for 192h;
DOI:10.1039/c39800000758

Reference yield:

: 3506-01-2
2'-Deoxyadenosine N¹-oxide

: 76227-21-9
N'-benzyloxy-1-(2-deoxy-β-D-ribofuranosyl)-5-formamido-1H-imidazole-4-carboxamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / AcNMe₂ / 4 h / Ambient temperature; 2.) H₂O, HClO₄

2: 70 percent / Amberlite IRA-402 (HClO₃^-) / H₂O

With N,N-dimethyl acetamide; Amberlite IRA-402 (HClO₃^-); In water;
DOI:10.1248/cpb.37.2601