(2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

Base Information

Chemical Name:(2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine
CAS No.:96034-97-8
Molecular Formula:C₁₆H₁₈N₂O₇S
Molecular Weight:382.394
Hs Code.:

Synonyms:(2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

Suppliers and Price of (2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

Chemical Property:

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Technology Process of (2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

There total 2 articles about (2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 138324-82-0
(2S,4R)-4-mesyloxy-1-(p-nitrobenzyloxycarbonyl)pyrrolidine-2-carboxylic acid methyl ester

: 10387-40-3
potassium thioacetate

: 96034-97-8
(2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

Guidance literature:: In N,N-dimethyl-formamide; at 50 ℃; for 10h;

Reference yield:

: 101803-29-6
(2S,4R)-4-hydroxy-2-methoxycarbonyl-1-(4-nitrobenzyloxycarbonyl)pyrrolidine

: 96034-97-8
(2S,4S)-4-acetylthio-2-methoxycarbonyl-1-p-nitrobenzyloxycarbonylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.08 h / -5 °C

2: N,N-dimethyl-formamide / 10 h / 50 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;