κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

Base Information

Chemical Name:κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)
CAS No.:128467-35-6
Molecular Formula:C₂₂H₁₇ClN₂Pt
Molecular Weight:539.923
Hs Code.:

κ<sup>2</sup>(N^C<sup>2</sup>)-(2-phenylpyridine)-κ<sup>1</sup>(N)-(2-phenylpyridine)chloro platinum(II)

Synonyms:κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

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Chemical Property of κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

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Technology Process of κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

There total 5 articles about κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.2%

: 1008-89-5
2-phenylpyridine

: 10025-99-7
potassium tetrachloroplatinate(II)

: 128467-35-6
κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

Guidance literature:: In water; (Ar), Pt complex treated with 3:1 mixt. of degassed ethoxyethanol and H2O, stirred for 10 min, treated with 2.2 equiv. of ligand, heated at 80°C, stirred for 16 h; evapd.(vac.), treated with CH3OH, stirred for 10 min at room temp., washed (CH3OH, n-pentane), dried (vac.), elem. anal.;
DOI:10.1016/j.ica.2007.02.001

Reference yield: 66.0%

: 1008-89-5
2-phenylpyridine

: 10025-99-7
potassium tetrachloroplatinate(II)

: 155475-93-7
phenylpyridinebridgedichloro platinum

: 128467-35-6
κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

Guidance literature:: In 2-ethoxy-ethanol; water; (N2), stoich., to aq. soln. of Pt complex added 2-phenylpyridine in 2-ethoxyethanole, heated at 70°C for 8 h; filtered, washed (H2O, acetone, CH2Cl2), washings dried, elem. anal.;
DOI:10.1016/j.jorganchem.2010.01.035

Reference yield:

: 155475-93-7
phenylpyridinebridgedichloro platinum

: 128467-35-6
κ²(N^C²)-(2-phenylpyridine)-κ¹(N)-(2-phenylpyridine)chloro platinum(II)

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide

2: dimethyl sulfoxide

In dimethyl sulfoxide;
DOI:10.1016/j.jorganchem.2010.01.035