VCl₃(N-4-MeC₆H₄)

Base Information

Chemical Name:VCl₃(N-4-MeC₆H₄)
CAS No.:90941-76-7
Molecular Formula:C₇H₇Cl₃NV
Molecular Weight:262.44
Hs Code.:

VCl<sub>3</sub>(N-4-MeC<sub>6</sub>H<sub>4</sub>)

Synonyms:VCl₃(N-4-MeC₆H₄)

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Chemical Property of VCl₃(N-4-MeC₆H₄)

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Technology Process of VCl₃(N-4-MeC₆H₄)

There total 1 articles about VCl₃(N-4-MeC₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7727-18-6
vanadium(V) oxychloride

: 622-58-2,374675-64-6
p-Tolylisocyanate

: 90941-76-7
VCl₃(N-4-MeC₆H₄)

Guidance literature:: In octane; (N2); soln. of V compd. and ligand refluxed for 3 h; soln. evapd. to dryness, residue dried in vac. for 18 h at 70°C and sublimed at 110°C/E-4 Torr; elem. anal.;
DOI:10.1021/ja00258a026

Reference yield: 94.0%

: 90941-76-7
VCl₃(N-4-MeC₆H₄)

: 75-05-8,26809-02-9
acetonitrile

: [VOCl₃(NCMe)2]*[p-tolylNH₃]

Guidance literature:: In acetonitrile; (N2); vanadium complex was refluxed in MeCN; cooled, evapd. in vac., elem. anal.;
DOI:10.1039/b901810g

Reference yield: 83.0%

: 90941-76-7
VCl₃(N-4-MeC₆H₄)

: tetra-phenol α,α,α’,α’-tetrakis(3,5-di-tert-butyl-2-hydroxyphenyl)-p-xylene

: C₈₆H₁₁₆Cl₂N₂O₆V₂*CH₂Cl₂

Guidance literature:: tetra-phenol α,α,α’,α’-tetrakis(3,5-di-tert-butyl-2-hydroxyphenyl)-p-xylene; With sodium; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

VCl₃(N-4-MeC₆H₄); In tetrahydrofuran; at -78 - 20 ℃; for 12h;
DOI:10.1039/c5ra20177b