(S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

Base Information

Chemical Name:(S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester
CAS No.:241496-50-4
Molecular Formula:C₁₂H₁₈NO₅P
Molecular Weight:287.252
Hs Code.:

Synonyms:(S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

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Chemical Property of (S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

Chemical Property:

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Technology Process of (S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

There total 6 articles about (S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: dimethyl α-((benzyloxycarbonyl)amino)ethenephosphonate

: 241496-50-4
(S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

Guidance literature:: With hydrogen; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In dichloromethane; at 20 ℃; for 24h; under 7600.51 Torr;
DOI:10.1021/jo702488j

Reference yield:

: 82629-22-9
1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

: 121843-85-4
(R)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

: 241496-50-4
(S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

: 145240-97-7
(R)-1-aminoethylphosphonic acid dimethyl ester

Guidance literature:: With penicillin G acylase from Escherichia coli; In aq. phosphate buffer; at 25 ℃; for 144h; pH=7; enantioselective reaction; Kinetics; Enzymatic reaction;
DOI:10.1016/j.molcatb.2016.05.011

Reference yield:

: [1-(N-benzyloxycarbonylamino)ethyl]triphenylphosphonium tetrafluoroborate

: 868-85-9
Dimethyl phosphite

: 121843-85-4
(R)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

: 241496-50-4
(S)-1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

Guidance literature:: [1-(N-benzyloxycarbonylamino)ethyl]triphenylphosphonium tetrafluoroborate; With C₂₇H₃₂FN₂O₂⁽¹⁺⁾*Br^(1-); In toluene; for 0.166667h; Sonication;

Dimethyl phosphite; With potassium hydroxide; In toluene; at -70 ℃; for 72h; Reagent/catalyst; Overall yield = 48.4 mg; enantioselective reaction;
DOI:10.3390/molecules25020405