C₂₃H₁₇F₂N₃O₄

Base Information

Chemical Name:C₂₃H₁₇F₂N₃O₄
CAS No.:1220124-87-7
Molecular Formula:C₂₃H₁₇F₂N₃O₄
Molecular Weight:437.402
Hs Code.:

C<sub>23</sub>H<sub>17</sub>F<sub>2</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₃H₁₇F₂N₃O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₇F₂N₃O₄

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Technology Process of C₂₃H₁₇F₂N₃O₄

There total 3 articles about C₂₃H₁₇F₂N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 66648-38-2
2,6-difluoro-hippuric acid

: 1224962-94-0
C₁₄H₁₄N₂O₃

: 1220124-87-7
C₂₃H₁₇F₂N₃O₄

Guidance literature:: 2,6-difluoro-hippuric acid; C₁₄H₁₄N₂O₃; With sodium acetate; In 2-methyltetrahydrofuran; at 55 ℃; for 0.5h;

With acetic anhydride; In 2-methyltetrahydrofuran; Reflux;
DOI:10.1021/op100032s

Reference yield:

: 219140-32-6
C₁₁H₁₁F₂NO₃

: 1220124-87-7
C₂₃H₁₇F₂N₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / 2-methyltetrahydrofuran / 1 h / 25 - 28 °C

2.1: sodium acetate / 2-methyltetrahydrofuran / 0.5 h / 55 °C

2.2: Reflux

With water; sodium acetate; sodium hydroxide; In 2-methyltetrahydrofuran;
DOI:10.1021/op100032s

Reference yield:

: 18063-02-0
2,6-difluorobenzoylchloride

: 1220124-87-7
C₂₃H₁₇F₂N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / 2-methyltetrahydrofuran; water / 0.5 h / Cooling

1.2: 3 h / 10 °C / Cooling

2.1: water; sodium hydroxide / 2-methyltetrahydrofuran / 1 h / 25 - 28 °C

3.1: sodium acetate / 2-methyltetrahydrofuran / 0.5 h / 55 °C

3.2: Reflux

With water; sodium acetate; sodium hydrogencarbonate; sodium hydroxide; In 2-methyltetrahydrofuran; water; 1.2: Schotten-Baumann reaction;
DOI:10.1021/op100032s