4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester

Base Information

Chemical Name:4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester
CAS No.:74670-92-1
Molecular Formula:C₁₅H₁₉BrO₄S
Molecular Weight:375.283
Hs Code.:

Synonyms:4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester

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Chemical Property of 4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester

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Technology Process of 4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester

There total 3 articles about 4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 497-38-1
Norbornan-2-on

: 74670-92-1
4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) HCl / 1.) THF, -78 deg C, 15 min, 2.) H₂O, room temperature

2: 85 percent / LiAlH₄ / diethyl ether / 6 h / Heating

3: pyridine / 19 h

With hydrogenchloride; lithium aluminium tetrahydride; In pyridine; diethyl ether;
DOI:10.1021/ja00539a014

Reference yield:

: 72055-12-0,144657-45-4,145575-95-7,145576-12-1
ethyl exo-(2-hydroxynorbornan-2-yl)acetate

: 74670-92-1
4-Bromo-benzenesulfonic acid 2-((1R,2R,4S)-2-hydroxy-bicyclo[2.2.1]hept-2-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / LiAlH₄ / diethyl ether / 6 h / Heating

2: pyridine / 19 h

With lithium aluminium tetrahydride; In pyridine; diethyl ether;
DOI:10.1021/ja00539a014