3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

Base Information

Chemical Name:3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester
CAS No.:114393-52-1
Molecular Formula:C₁₃H₁₄N₂O₂S₃
Molecular Weight:326.464
Hs Code.:

Synonyms:3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

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Chemical Property of 3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

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Technology Process of 3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

There total 5 articles about 3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114392-96-0
2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

: 140-88-5,9003-32-1
ethyl acrylate

: 114393-52-1
3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

Guidance literature:: With thionyl chloride; triethylamine; Yield given. Multistep reaction; 1) benzene, reflux, 18 h; 2) methylene chloride, reflux, 2 h;

Reference yield:

: 78365-67-0
N-<2-(phenylthio)acetyl>piperidine

: 114393-52-1
3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / bis(4-methoxyphenyl)-1,3,2,4-dithiaphosphetane-2,4-disulfide (Lawesson Reagent) / toluene / 6 h / Heating

2: benzene / 12 h / Ambient temperature

3: H₂S / ethanol / 6 h / Heating

4: 65 percent / CH₂Cl₂ / 2 h / Heating

5: 1) triethylamine; 2) thionyl chloride / 1) benzene, reflux, 18 h; 2) methylene chloride, reflux, 2 h

With Lawessons reagent; thionyl chloride; hydrogen sulfide; triethylamine; In ethanol; dichloromethane; toluene; benzene;

Reference yield:

: 114392-97-1
N-<2-(Phenylthio)-1-thioxoethyl>piperidine

: 114393-52-1
3-[[5-(Phenylthio)-1,2,3-thiadiazol-4-yl]thio]propanoic acid, ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 12 h / Ambient temperature

2: H₂S / ethanol / 6 h / Heating

3: 65 percent / CH₂Cl₂ / 2 h / Heating

4: 1) triethylamine; 2) thionyl chloride / 1) benzene, reflux, 18 h; 2) methylene chloride, reflux, 2 h

With thionyl chloride; hydrogen sulfide; triethylamine; In ethanol; dichloromethane; benzene;