2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

Base Information

Chemical Name:2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester
CAS No.:114392-96-0
Molecular Formula:C₁₀H₁₂N₂O₂S₂
Molecular Weight:256.349
Hs Code.:

Synonyms:2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

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Chemical Property of 2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

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Technology Process of 2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

There total 5 articles about 2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 6294-89-9
hydrazinecarboxylic acid methyl ester

: 122483-67-4
Ethyl <(2-Phenylthio-1-thioxoethyl)thio>acetate

: 114392-96-0
2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

Guidance literature:: In dichloromethane; for 2h; Heating;

Reference yield:

: 78365-67-0
N-<2-(phenylthio)acetyl>piperidine

: 114392-96-0
2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / bis(4-methoxyphenyl)-1,3,2,4-dithiaphosphetane-2,4-disulfide (Lawesson Reagent) / toluene / 6 h / Heating

2: benzene / 12 h / Ambient temperature

3: H₂S / ethanol / 6 h / Heating

4: 65 percent / CH₂Cl₂ / 2 h / Heating

With Lawessons reagent; hydrogen sulfide; In ethanol; dichloromethane; toluene; benzene;

Reference yield:

: 114392-97-1
N-<2-(Phenylthio)-1-thioxoethyl>piperidine

: 114392-96-0
2-[2-(phenylthio)-1-thioxoethyl]hydrazinecarboxylic acid, methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 12 h / Ambient temperature

2: H₂S / ethanol / 6 h / Heating

3: 65 percent / CH₂Cl₂ / 2 h / Heating

With hydrogen sulfide; In ethanol; dichloromethane; benzene;