1-[(2-Methoxyethoxy)methyl]-6-phenylthiothymine

Base Information

Chemical Name:1-[(2-Methoxyethoxy)methyl]-6-phenylthiothymine
CAS No.:132774-35-7
Molecular Formula:C15H18N2O4S
Molecular Weight:322.3794
Hs Code.:
Mol file:132774-35-7.mol

Synonyms:1-MeOEtOMe-6PhS T;

Suppliers and Price of 1-[(2-Methoxyethoxy)methyl]-6-phenylthiothymine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-[(2-Methoxyethoxy)methyl]-6-phenylthiothymine

Chemical Property:

PSA：98.88000
Density:1.3g/cm³
LogP:2.02900

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-[(2-Methoxyethoxy)methyl]-6-phenylthiothymine

There total 3 articles about 1-[(2-Methoxyethoxy)methyl]-6-phenylthiothymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132774-47-1
1-<(2-methoxyethoxy)methyl>-thymine

: 882-33-7
diphenyldisulfane

: 132774-35-7
1-<(2-methoxyethoxy)methyl>-6-(phenylthio)thymine

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -70 deg C, 1 h, 2.) THF, 40 min;
DOI:10.1021/jm00108a041

Reference yield:

: 65-71-4,28806-14-6,691841-57-3
thymin

: 132774-35-7
1-<(2-methoxyethoxy)methyl>-6-(phenylthio)thymine

Guidance literature:: Multi-step reaction with 3 steps

1: (NH₄)2SO₄ / Heating

2: NaI / 1,2-dichloro-ethane / 3 h / Heating

3: 1.) LDA / 1) THF, below -70 deg C, 1.5 h; 2) THF, below -70 deg C, 30 min

With ammonium sulfate; sodium iodide; lithium diisopropyl amide; In 1,2-dichloro-ethane;
DOI:10.1080/00397919908085786

Reference yield:

: 7288-28-0
2,4-bis(trimethylsiloxy)-5-methylpyrimidine

: 132774-35-7
1-<(2-methoxyethoxy)methyl>-6-(phenylthio)thymine

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / 1,2-dichloro-ethane / 3 h / Heating

2: 1.) LDA / 1) THF, below -70 deg C, 1.5 h; 2) THF, below -70 deg C, 30 min

With sodium iodide; lithium diisopropyl amide; In 1,2-dichloro-ethane;
DOI:10.1080/00397919908085786