2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

Base Information

Chemical Name:2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester
CAS No.:1256358-40-3
Molecular Formula:C₂₉H₂₇OPS
Molecular Weight:454.573
Hs Code.:

Synonyms:2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

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Chemical Property of 2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

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Technology Process of 2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

There total 1 articles about 2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 1247748-11-3
S-2,6-dimethylphenyl α-bromothiopropionate

: 603-35-0
triphenylphosphine

: 1256358-40-3
2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

Guidance literature:: In benzene; for 3h; Reflux;
DOI:10.1021/ol102407k

Reference yield: 91.0%

: 1256358-40-3
2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

: 582-24-1
1-phenyl-2-hydroxyethanone

: 1575-48-0
3-methyl-4-phenylfuran-2(5H)-one

Guidance literature:: With Oxone; C₈H₆O₄^(2-)*Cu⁽²⁺⁾; In toluene; at 60 ℃; for 9h; Molecular sieve;
DOI:10.1021/ol102407k

Reference yield: 81.0%

: 1256358-40-3
2-(triphenylphosphoranylidene)propanethioic acid S-(2,6-dimethylphenyl) ester

: 130921-11-8,130921-12-9,477199-83-0
(±)-2-hydroxy-6-methoxy-4,7-dimethyl-3,4-dihydronaphthalen-1(2H)-one

: 123914-48-7,130982-23-9,130982-24-0
(+/-)-8-epi-heritol methyl ether

: 123914-48-7,130982-23-9,130982-24-0
(+/-)-Methyl heritol

Guidance literature:: With Oxone; C₈H₆O₄^(2-)*Cu⁽²⁺⁾; In 5,5-dimethyl-1,3-cyclohexadiene; toluene; at 60 - 138 ℃; for 11h; optical yield given as %de; Molecular sieve;
DOI:10.1021/ol102407k