4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

Base Information

Chemical Name:4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde
CAS No.:1384262-19-4
Molecular Formula:C₄₉H₄₂N₂OS₂
Molecular Weight:739.017
Hs Code.:

Synonyms:4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

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Chemical Property of 4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

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Technology Process of 4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

There total 2 articles about 4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1384262-18-3
4-(5-(5-(5-bromothiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1384262-19-4
4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 48h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.04.104

Reference yield:

: 1236309-06-0
1-(2,6-diisopropylphenyl)-2,5-di(thiophen-2-yl)-1H-pyrrole

: 1384262-19-4
4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 6 h / 0 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 48 h / Inert atmosphere; Reflux

3: N-Bromosuccinimide / N,N-dimethyl-formamide / 6 h / 0 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 48 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 2: Suzuki coupling / 4: Suzuki coupling;
DOI:10.1016/j.tet.2012.04.104

Reference yield: 88.0%

: 1384262-19-4
4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde

: 372-09-8
cyanoacetic acid

: 1384262-13-8
(E)-3-(4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)phenyl)-2-cyanoacrylic acid

Guidance literature:: 4-(5-(5-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)-1-(2,6-diisopropylphenyl)-1H-pyrrol-2-yl)thiophen-2-yl)benzaldehyde; cyanoacetic acid; With piperidine; In chloroform; acetonitrile; for 18h; Reflux;

With hydrogenchloride; In dichloromethane; water;
DOI:10.1016/j.tet.2012.04.104