C₃₁H₅₀O₈Si

Base Information

Chemical Name:C₃₁H₅₀O₈Si
CAS No.:250577-83-4
Molecular Formula:C₃₁H₅₀O₈Si
Molecular Weight:578.819
Hs Code.:

C<sub>31</sub>H<sub>50</sub>O<sub>8</sub>Si

Synonyms:C₃₁H₅₀O₈Si

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Chemical Property of C₃₁H₅₀O₈Si

Chemical Property:

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Technology Process of C₃₁H₅₀O₈Si

There total 18 articles about C₃₁H₅₀O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 250577-76-5
C₃₂H₅₀O₉Si

: 250577-83-4
C₃₁H₅₀O₈Si

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 0.0833333h;
DOI:10.1021/ol990281j

Reference yield:

: 250577-77-6
C₃₁SiH₄₀O₄

: 250577-83-4
C₃₁H₅₀O₈Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

3.1: 3.39 g / toluene / 1 h / 70 °C

4.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

6.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

7.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

8.1: 98 percent / benzene / 14 h / Heating

9.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

9.2: 78 percent / tetrahydrofuran / -78 - 20 °C

10.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

11.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

With oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 2.1: Swern oxidation / 3.1: Wittig olefination / 4.2: Wittig olefination / 10.1: Wittig olefination;
DOI:10.1021/ol990281j

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 250577-83-4
C₃₁H₅₀O₈Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: 98 percent / imidazole / dimethylformamide / 0.5 h / 20 °C

2.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

3.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

4.1: 3.39 g / toluene / 1 h / 70 °C

5.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

5.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

6.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

7.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

8.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

9.1: 98 percent / benzene / 14 h / Heating

10.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

10.2: 78 percent / tetrahydrofuran / -78 - 20 °C

11.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

12.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

With 1H-imidazole; oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; benzene; 3.1: Swern oxidation / 4.1: Wittig olefination / 5.2: Wittig olefination / 11.1: Wittig olefination;
DOI:10.1021/ol990281j