Technology Process of C28H33Cl2N3O6
There total 15 articles about C28H33Cl2N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 9 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 19 h / 65 °C
3.1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / acetonitrile; water / 24.5 h / 15 - 20 °C
4.1: thionyl chloride / 6 h / Reflux
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C
5.2: 1.5 h / 10 - 20 °C
6.1: hydrazine hydrate / ethanol / 2 h / Reflux
7.1: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C
8.1: ammonium fluoride / water; ethanol / 48 h / 45 °C
9.1: hydrogenchloride / water; ethanol / 12 h / 20 °C
With
hydrogenchloride; ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; dihydrogen peroxide; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.058
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 19 h / 65 °C
2.1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / acetonitrile; water / 24.5 h / 15 - 20 °C
3.1: thionyl chloride / 6 h / Reflux
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C
4.2: 1.5 h / 10 - 20 °C
5.1: hydrazine hydrate / ethanol / 2 h / Reflux
6.1: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C
7.1: ammonium fluoride / water; ethanol / 48 h / 45 °C
8.1: hydrogenchloride / water; ethanol / 12 h / 20 °C
With
hydrogenchloride; ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; dihydrogen peroxide; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.058