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C28H33Cl2N3O6

Base Information
  • Chemical Name:C28H33Cl2N3O6
  • CAS No.:1424337-12-1
  • Molecular Formula:C28H33Cl2N3O6
  • Molecular Weight:578.493
  • Hs Code.:
C<sub>28</sub>H<sub>33</sub>Cl<sub>2</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C28H33Cl2N3O6

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Chemical Property of C28H33Cl2N3O6
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Technology Process of C28H33Cl2N3O6

There total 15 articles about C28H33Cl2N3O6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; In ethanol; water; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2012.11.058
Guidance literature:
Multi-step reaction with 9 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 19 h / 65 °C
3.1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / acetonitrile; water / 24.5 h / 15 - 20 °C
4.1: thionyl chloride / 6 h / Reflux
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C
5.2: 1.5 h / 10 - 20 °C
6.1: hydrazine hydrate / ethanol / 2 h / Reflux
7.1: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C
8.1: ammonium fluoride / water; ethanol / 48 h / 45 °C
9.1: hydrogenchloride / water; ethanol / 12 h / 20 °C
With hydrogenchloride; ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; dihydrogen peroxide; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.058
Guidance literature:
Multi-step reaction with 8 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 19 h / 65 °C
2.1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / acetonitrile; water / 24.5 h / 15 - 20 °C
3.1: thionyl chloride / 6 h / Reflux
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C
4.2: 1.5 h / 10 - 20 °C
5.1: hydrazine hydrate / ethanol / 2 h / Reflux
6.1: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C
7.1: ammonium fluoride / water; ethanol / 48 h / 45 °C
8.1: hydrogenchloride / water; ethanol / 12 h / 20 °C
With hydrogenchloride; ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; dihydrogen peroxide; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.058
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