Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

Base Information

Chemical Name:Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester
CAS No.:15929-45-0
Molecular Formula:C₁₈H₁₃Cl₂OPS
Molecular Weight:379.246
Hs Code.:

Synonyms:Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

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Technology Process of Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

There total 3 articles about Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15948-60-4
bis(4-chlorophenyl)phosphine oxide

: 108-98-5
thiophenol

: 15929-45-0
Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

Guidance literature:: With tert-Butyl peroxybenzoate; potassium iodide; In dimethyl sulfoxide; at 20 ℃; for 8h;
DOI:10.1039/c4gc00944d

Reference yield:

: 15948-60-4
bis(4-chlorophenyl)phosphine oxide

: 882-33-7
diphenyldisulfane

: 15929-45-0
Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

Guidance literature:: With hydroquinone; In tert-butyl alcohol;
DOI:10.1016/0040-4020(67)85057-9

Reference yield:

: 106-39-8
bromochlorobenzene

: 15929-45-0
Bis-(p-chlor-phenyl)-thiolphosphinsaeure-phenylester

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium / tetrahydrofuran / 20 °C

1.2: -15 - 20 °C

2.1: tert-Butyl peroxybenzoate; potassium iodide / dimethyl sulfoxide / 8 h / 20 °C

With tert-Butyl peroxybenzoate; iodine; magnesium; potassium iodide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1039/c4gc00944d