Technology Process of C24H28Cl2O6S
There total 7 articles about C24H28Cl2O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; pyridinium p-toluenesulfonate;
at 20 - 40 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C
2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 6 h
3: triethylamine / dichloromethane / 0 - 20 °C
4: tetrabutyl-ammonium chloride / toluene / 18 h / 40 °C
5: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C
6: methanol / pyridinium p-toluenesulfonate / 20 - 40 °C
With
methanol; di-isopropyl azodicarboxylate; tetrabutyl-ammonium chloride; hydrogen; potassium carbonate; triethylamine; triphenylphosphine;
palladium 10% on activated carbon; pyridinium p-toluenesulfonate;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
5: Mitsunobu reaction;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 0 - 20 °C
2: tetrabutyl-ammonium chloride / toluene / 18 h / 40 °C
3: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C
4: methanol / pyridinium p-toluenesulfonate / 20 - 40 °C
With
methanol; di-isopropyl azodicarboxylate; tetrabutyl-ammonium chloride; triethylamine; triphenylphosphine;
pyridinium p-toluenesulfonate;
In
dichloromethane; toluene;
3: Mitsunobu reaction;