3-chloro-5-hydroxybenzyl acetate

Base Information Edit

Chemical Name:3-chloro-5-hydroxybenzyl acetate
CAS No.:899808-15-2
Molecular Formula:C₉H₉ClO₃
Molecular Weight:200.622
Hs Code.:
Mol file:899808-15-2.mol

Synonyms:3-chloro-5-hydroxybenzyl acetate

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Chemical Property of 3-chloro-5-hydroxybenzyl acetate Edit

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Technology Process of 3-chloro-5-hydroxybenzyl acetate

There total 5 articles about 3-chloro-5-hydroxybenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 899808-14-1
C₁₅H₂₃ClO₃Si

: 899808-15-2
3-chloro-5-hydroxybenzyl acetate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 899808-13-0
C₁₃H₂₁ClO₂Si

: 899808-15-2
3-chloro-5-hydroxybenzyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 899808-12-9
C₁₄H₂₁ClO₃Si

: 899808-15-2
3-chloro-5-hydroxybenzyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride / tetrahydrofuran / 0 °C / Reflux

1.2: Cooling with ice

2.1: pyridine / dichloromethane

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

With pyridine; lithium borohydride; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;