C₁₇H₂₄O₂Si

Base Information

Chemical Name:C₁₇H₂₄O₂Si
CAS No.:1535990-56-7
Molecular Formula:C₁₇H₂₄O₂Si
Molecular Weight:288.462
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>2</sub>Si

Synonyms:C₁₇H₂₄O₂Si

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Chemical Property of C₁₇H₂₄O₂Si

Chemical Property:

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Technology Process of C₁₇H₂₄O₂Si

There total 1 articles about C₁₇H₂₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 252949-41-0
C₁₆H₂₄OSi

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1535990-56-7
C₁₇H₂₄O₂Si

Guidance literature:: C₁₆H₂₄OSi; N,N-dimethyl-formamide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere; Large scale;

In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere; Large scale;
DOI:10.1021/jo4026868

Reference yield:

: 1535990-56-7
C₁₇H₂₄O₂Si

: C₁₇H₂₅NO₂Si

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 2h; Inert atmosphere; Large scale;
DOI:10.1021/jo4026868

Reference yield:

: 1535990-56-7
C₁₇H₂₄O₂Si

: 1535990-64-7
C₂₆H₄₀O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; hydroxylamine hydrochloride / ethanol / 2 h / 20 °C / Inert atmosphere; Large scale

2.1: tert-butylhypochlorite; triethylamine / ethanol; diethyl ether / -78 - 20 °C / Inert atmosphere; Large scale

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Large scale

4.1: samarium diiodide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Large scale

4.2: 0.5 h / 20 °C / Large scale

With pyridine; samarium diiodide; tert-butylhypochlorite; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/jo4026868