3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Base Information

Chemical Name:3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide
CAS No.:875557-17-8
Molecular Formula:C₂₃H₁₇N₃O₃
Molecular Weight:383.406
Hs Code.:

Synonyms:3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Suppliers and Price of 3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

There total 5 articles about 3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 100-52-7
benzaldehyde

: 875557-11-2
3-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid hydrazide

: 875557-17-8
3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: With acetic acid; for 4h; Heating;

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 875557-17-8
3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / H₂O; methanol / 2 h / Heating

2: 60 percent / H₂SO₄ / 1 h / 20 °C

3: PCl₅ / CCl₄ / 2 h / 100 °C

4: hydrazine hydrate / 5 h / 20 °C

5: 50 percent / acetic acid / 4 h / Heating

With phosphorus pentachloride; sulfuric acid; potassium carbonate; hydrazine hydrate; acetic acid; In methanol; tetrachloromethane; water;

Reference yield:

: 118-29-6
2-(hydroxymethyl)-1H-isoindole-1,3(2H)-dione

: 875557-17-8
3-(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / H₂SO₄ / 1 h / 20 °C

2: PCl₅ / CCl₄ / 2 h / 100 °C

3: hydrazine hydrate / 5 h / 20 °C

4: 50 percent / acetic acid / 4 h / Heating

With phosphorus pentachloride; sulfuric acid; hydrazine hydrate; acetic acid; In tetrachloromethane;