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p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide

Base Information
  • Chemical Name:p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide
  • CAS No.:159675-87-3
  • Molecular Formula:C29H29NO5
  • Molecular Weight:471.553
  • Hs Code.:
p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide

Synonyms:p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide

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Chemical Property of p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide
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Technology Process of p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide

There total 5 articles about p-Benzyloxycarbonyl-α-methylcinnamic acid N-ethoxycarbonylmethyl-N-phenylmethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1: 1.) sodium hydride / 1.) THF, 25 deg C, 30 min, 2.) THF, 25 deg C, 30 min
2: 84 percent / trifluoroacetic acid / various solvent(s) / 2 h
3: thionyl chloride / 1 h / Heating
4: pyridine / CH2Cl2 / 2 h / 25 °C
With pyridine; thionyl chloride; sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm00022a017
Guidance literature:
Multi-step reaction with 2 steps
1: thionyl chloride / 1 h / Heating
2: pyridine / CH2Cl2 / 2 h / 25 °C
With pyridine; thionyl chloride; In dichloromethane;
DOI:10.1021/jm00022a017
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