(1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

Base Information

Chemical Name:(1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate
CAS No.:111646-96-9
Molecular Formula:C₁₈H₂₆N₂O₃
Molecular Weight:318.416
Hs Code.:

(1R,2R,2'S,4E)-1-(N<sub>1</sub>,N<sub>2</sub>-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

Synonyms:(1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

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Chemical Property of (1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

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Technology Process of (1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

There total 5 articles about (1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 111610-38-9
(2R,5S,1'R,2'R)-5-((E)-1'-benzoyloxy-2'-methyl-4'-hexenyl)-2-(tert-butyl)-1,3-dimethylimidazolidin-4-one

: 111646-96-9
(1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

Guidance literature:: With hydrogenchloride; In ethanol; at 90 ℃; for 4h;
DOI:10.1002/hlca.19870700129

Reference yield:

: 104372-54-5,519002-37-0
(-)-(2R)-2-methyl-4-hexenal

: 111646-96-9
(1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / (i-Pr)2NH, BuLi / tetrahydrofuran; hexane / 1.) -75 degC, 20 min; 2.) -100 degC, 50 min; 3.) 30 min, r.t.

2: 84 percent / 40 percent aq. NaOH / acetone / 12 h / 50 °C

3: 100 percent / 2 N HCl / ethanol / 4 h / 90 °C

With hydrogenchloride; sodium hydroxide; n-butyllithium; diisopropylamine; In tetrahydrofuran; ethanol; hexane; acetone;
DOI:10.1002/hlca.19870700129

Reference yield:

: 98-88-4
benzoyl chloride

: 111646-96-9
(1R,2R,2'S,4E)-1-(N₁,N₂-dimethylglycinamide-2'-yl)-2-methyl-4-hexenyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

2: 82 percent / (i-Pr)2NH, BuLi / tetrahydrofuran; hexane / 1.) -75 degC, 20 min; 2.) -100 degC, 50 min; 3.) 30 min, r.t.

3: 84 percent / 40 percent aq. NaOH / acetone / 12 h / 50 °C

4: 100 percent / 2 N HCl / ethanol / 4 h / 90 °C

With hydrogenchloride; sodium hydroxide; n-butyllithium; diisopropylamine; In tetrahydrofuran; ethanol; hexane; acetone;
DOI:10.1002/hlca.19870700129