N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

Base Information

Chemical Name:N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine
CAS No.:1190833-68-1
Molecular Formula:C₄₈H₄₀N₄O₂S
Molecular Weight:736.937
Hs Code.:

Synonyms:N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

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Chemical Property of N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

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Technology Process of N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

There total 14 articles about N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1190833-67-0
7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

: 1190833-68-1
N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

Guidance literature:: With hydrazine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; at 60 ℃; for 8.66667h; Inert atmosphere;

Reference yield: 65.0%

: 1190833-67-0
7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

: 2-(9,9-Diethyl-2-fluorenyl)-benzothiazole

: C₂₄H₂₁NOS

: C₄₂H₃₅N₃O₂S

: 1190833-68-1
N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

Guidance literature:: With palladium 10% on activated carbon; hydrazine hydrate; In tetrahydrofuran; ethanol; at 60 ℃; for 8.66667h; Inert atmosphere;
DOI:10.1021/ma201407g

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1190833-68-1
N,N-bis(3-(4-aminophenoxy)phenyl)-7-(benzo[d]thiazol-2-yl)-9,9-diethyl-9H-fluoren-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl acetamide / 5 h / 97 °C

2: palladium 10% on activated carbon; hydrazine hydrate / tetrahydrofuran; ethanol / 8.67 h / 60 °C / Inert atmosphere

With palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; In tetrahydrofuran; ethanol; N,N-dimethyl acetamide;
DOI:10.1021/ma201407g