7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

Base Information

Chemical Name:7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine
CAS No.:1190833-67-0
Molecular Formula:C₄₈H₃₆N₄O₆S
Molecular Weight:796.903
Hs Code.:

Synonyms:7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

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Chemical Property of 7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

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Technology Process of 7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

There total 8 articles about 7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 701971-75-7
N,N-di(3-hydroxyphenyl)-7-(benzothiazol-2-yl)-9,9-diethylfluoren-2-amine

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1190833-67-0
7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

Guidance literature:: With potassium carbonate; In N,N-dimethyl acetamide; at 97 ℃; for 5h;
DOI:10.1021/ma201407g

Reference yield:

: 225113-41-7
2-(7-bromo-9,9-diethyl-9H-fluoren-2-yl)benzothiazole

: 1190833-67-0
7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate / toluene / 24 h / 100 °C / Inert atmosphere

2: pyridine hydrochloride / 10 h / 200 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl acetamide / 5 h / 97 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; pyridine hydrochloride; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In N,N-dimethyl acetamide; toluene;
DOI:10.1021/ma201407g

Reference yield:

: 701971-73-5
N,N-di(3-methoxyphenyl)-7-(benzothiazol-2-yl)-9,9-diethylfluoren-2-amine

: 1190833-67-0
7-(benzo[d]thiazol-2-yl)-9,9-diethyl-N,N-bis(3-(4-nitrophenoxy)phenyl)-9H-fluoren-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / 10 h / 200 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl acetamide / 5 h / 97 °C

With pyridine hydrochloride; potassium carbonate; In N,N-dimethyl acetamide;
DOI:10.1021/ma201407g