1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

Base Information

Chemical Name:1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol
CAS No.:669713-10-4
Molecular Formula:C₈₆H₉₉N₃O₁₆Si
Molecular Weight:1458.83
Hs Code.:

1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

Synonyms:1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

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Chemical Property of 1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

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Technology Process of 1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

There total 1 articles about 1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 491869-97-7
1,2-O-cyclohexylidene-3,4,5-tri-O-benzyl-6-O-(2-azido-3,6-di-O-benzyl-2-deoxy-4-α-D-glucopyranosyl)-D-myo-inositol

: ((3aS,5R,6R,7S,7aS)-6,7-Bis-benzyloxy-2-pent-4-enyloxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran-5-ylmethoxy)-tert-butyl-dimethyl-silane

: 669713-10-4
1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

Guidance literature:: With N-iodo-succinimide; boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃;
DOI:10.1021/ja038807p

Reference yield:

: 100-39-0
benzyl bromide

: 669713-10-4
1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

: 669706-07-4
1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol

Guidance literature:: 1,2-O-cyclohexylidene-O-3,4,5-tri-O-benzyl-6-O-{(2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-(1->4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)}-D-myo-inositol; With sodium methylate; In methanol; dichloromethane;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; sodium hydride; In dichloromethane; Further stages.;
DOI:10.1016/j.tetlet.2003.10.179