1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

Base Information

Chemical Name:1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate
CAS No.:1408232-02-9
Molecular Formula:CF₃O₃S*C₁₇H₂₇N₃P
Molecular Weight:453.466
Hs Code.:

Synonyms:1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

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Technology Process of 1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

There total 1 articles about 1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 39106-95-1
di-tert-butylphosphanylbromide

: 2926-30-9
sodium triflate

: 3357-31-1
4-methyl-3-phenyl-4H-1,2,4-triazole

: 1408232-02-9
1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/om300872g

Reference yield: 70.0%

: 1408232-02-9
1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

: 1408232-03-0
1-(di-tert-butylphosphino)-4-methyl-3-phenyl-1,2,4-triazol-5-ylidene

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -95 - 20 ℃; Inert atmosphere;
DOI:10.1021/om300872g

Reference yield:

: 1408232-02-9
1-(di-tert-butylphosphino)-4-methyl-3-phenyl-4H-1,2,4-triazol-1-ium trifluoromethanesulfonate

: 1408232-04-1
3-(di-tert-butylphosphino)-4-methyl-5-phenyl-4H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hexamethyldisilazane / tetrahydrofuran / -95 - 20 °C / Inert atmosphere

2: benzene / 0.83 h / 90 °C / Inert atmosphere

With sodium hexamethyldisilazane; In tetrahydrofuran; benzene;
DOI:10.1021/om300872g