2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

Base Information

Chemical Name:2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine
CAS No.:934472-10-3
Molecular Formula:C₂₀H₃₅NO₃SSi
Molecular Weight:397.654
Hs Code.:

Synonyms:2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

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Chemical Property of 2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

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Technology Process of 2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

There total 7 articles about 2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1130814-69-5
2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine

: 934472-10-3
2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 3h;
DOI:10.1002/jccs.200800063

Reference yield: 80.0%

: 934472-09-0
N-{1-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-5-hydroxy-pentyl}-4-methyl-benzenesulfonamide

: 934472-10-3
2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 8h;
DOI:10.1016/j.tetlet.2007.01.082

Reference yield:

: 934472-06-7
2-hydroxyethyl-1-(toluene-4-sulfonyl)aziridine

: 934472-10-3
2-(1-t-butyldimethylsilyloxyethyl)-1-(4-methylphenylsulfonyl)-piperidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: imidazole / tetrahydrofuran / 8 h / 0 - 20 °C

2.1: 82 percent / tetrahydrofuran; diethyl ether / 6 h / -78 - 20 °C

3.1: BH₃*DMS / tetrahydrofuran / 8 h / -10 - 20 °C

3.2: 82 percent / H₂O₂; NaOH / 2 h / 0 - 20 °C

4.1: 80 percent / diisopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 8 h / 0 - 20 °C

With 1H-imidazole; di-isopropyl azodicarboxylate; dimethylsulfide borane complex; triphenylphosphine; In tetrahydrofuran; diethyl ether; 4.1: Mitsunobu condensation;
DOI:10.1016/j.tetlet.2007.01.082