(2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

Base Information

Chemical Name:(2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one
CAS No.:208512-14-5
Molecular Formula:C₂₃H₂₇N₃O₂S₂
Molecular Weight:441.618
Hs Code.:

Synonyms:(2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

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Chemical Property of (2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

Chemical Property:

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Technology Process of (2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

There total 2 articles about (2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 208512-12-3
(4S,5R)-(-)-1-[2'-[bis(methylsulfanyl)methylene]aminoacetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

: (2R,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

: 208512-14-5
(2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

Guidance literature:: With potassium tert-butylate; lithium chloride; lithium iodide; In tetrahydrofuran; at -78 - -20 ℃; for 2.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(98)00113-X

Reference yield:

: 620-05-3
iodomethylbenzene

: 208512-12-3
(4S,5R)-(-)-1-[2'-[bis(methylsulfanyl)methylene]aminoacetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

: (2R,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

: 208512-14-5
(2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

Guidance literature:: With lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 0 ℃; for 2.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(98)00113-X

Reference yield: 36.0%

: 208512-14-5
(2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

Guidance literature:: (2S,4'S,5'R)-1-(3',4'-dimethyl-2'-oxo-5'-phenyl-1'-imidazolydinyl)-2-[bis(methylsulfanyl)methyleneamino]-3-phenylpropan-1-one; With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 12h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 24h; Further stages.;
DOI:10.1021/jo000321t