(S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

Base Information

Chemical Name:(S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate
CAS No.:1201946-64-6
Molecular Formula:C₂₂H₁₉ClN₂O₄S
Molecular Weight:442.923
Hs Code.:

Synonyms:(S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

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Chemical Property of (S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

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Technology Process of (S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

There total 5 articles about (S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1201946-64-6
(S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

Guidance literature:

Reference yield: 38.8%

: 10400-19-8
3-pyridinecarbonyl chloride

: 1147350-75-1,109904-27-0
2-Oxoclopidogrel

: 1201946-64-6
(S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

Guidance literature:: 2-Oxoclopidogrel; With triethylamine; In tetrahydrofuran; for 0.166667h;

3-pyridinecarbonyl chloride; In tetrahydrofuran; at 0 - 25 ℃; for 4h;
DOI:10.1021/jm300038c

Reference yield: 17.1%

: 10400-19-8
3-pyridinecarbonyl chloride

: 527687-26-9
S(+)-2-(2-chlorophenyl)-2-(4,5,6,7-tetrahydro-thieno[3,2-c]pyridine-2(4H)-one)-5-acetic acid methyl ester

: 5538-51-2
O-acetylsalicyloyl chloride

: 1201946-64-6
(S)-5-(1-(2-chlorophenyl)-2-methoxy-2-oxoethyl)-4,5,6,7-tetrahydrothieno[3,2-c]pyridin-2-yl nicotinate

Guidance literature:: 3-pyridinecarbonyl chloride; S(+)-2-(2-chlorophenyl)-2-(4,5,6,7-tetrahydro-thieno[3,2-c]pyridine-2(4H)-one)-5-acetic acid methyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.5h;

O-acetylsalicyloyl chloride; In tetrahydrofuran; mineral oil; for 2h;