N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

Base Information

Chemical Name:N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide
CAS No.:796863-51-9
Molecular Formula:C₂₂H₂₈N₂O₃
Molecular Weight:368.476
Hs Code.:

Synonyms:N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

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Technology Process of N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

There total 3 articles about N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 796863-50-8
N-[4-[(3-methylphenyl)hydroxymethyl]-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

: 796863-51-9
N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

Guidance literature:: With manganese(IV) oxide; In toluene; Heating;
DOI:10.1021/jm0407658

Reference yield:

: 620-23-5
m-tolyl aldehyde

: 796863-51-9
N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; TMEDA / tetrahydrofuran; hexane / -78 - 0 °C

1.2: 70 percent / tetrahydrofuran; hexane / -78 - 0 °C

2.1: 92 percent / MnO₂ / toluene / Heating

With manganese(IV) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/jm0407658

Reference yield:

: 197229-98-4
5-ethyl-2-methoxy-6-methyl-3-pivaloylaminopyridine

: 796863-51-9
N-[4-(3-methylbenzoyl)-5-ethyl-2-methoxy-6-methylpyridin-3-yl]-2,2-dimethylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; TMEDA / tetrahydrofuran; hexane / -78 - 0 °C

1.2: 70 percent / tetrahydrofuran; hexane / -78 - 0 °C

2.1: 92 percent / MnO₂ / toluene / Heating

With manganese(IV) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/jm0407658