(2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

Base Information

Chemical Name:(2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine
CAS No.:917477-93-1
Molecular Formula:C₃₆H₂₆O₂P₂
Molecular Weight:552.549
Hs Code.:

Synonyms:(2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

Suppliers and Price of (2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

Chemical Property:

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Technology Process of (2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

There total 3 articles about (2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 22749-43-5
p-chlorodibenzo[c.e][1,2]oxaphosphorine

: 155566-51-1
2'-hydroxy-2-diphenylphosphinobiphenyl

: 917477-93-1
(2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

Guidance literature:: With triethylamine; In toluene; at 26 ℃; for 3h;
DOI:10.1016/j.jorganchem.2006.08.080

Reference yield:

: 22749-43-5
p-chlorodibenzo[c.e][1,2]oxaphosphorine

: 917477-93-1
(2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran / 20 h / 26 °C

2: 72 percent / triethylamine / toluene / 3 h / 26 °C

With triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/j.jorganchem.2006.08.080

Reference yield:

: phenylmagnesium bromide

: 917477-93-1
(2'-diphenylphosphino-biphenyl-2-yl)-oxydibenzo[c.e][5,6]oxaphosphorine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran / 20 h / 26 °C

2: 72 percent / triethylamine / toluene / 3 h / 26 °C

With triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/j.jorganchem.2006.08.080