3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

Base Information

Chemical Name:3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one
CAS No.:1186018-78-9
Molecular Formula:C₂₆H₃₂O₈
Molecular Weight:472.535
Hs Code.:

Synonyms:3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

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Chemical Property of 3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

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Technology Process of 3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

There total 5 articles about 3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 13709-06-3
2,4-bis(methoxymethoxy)benzaldehyde

: 99217-72-8
2-hydroxy-5-(3,3-dimethylallyl)-4-methoxymethyloxyacetophenone

: 1186018-78-9
3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

Guidance literature:: With potassium hydroxide; In ethanol; water; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1002/ardp.200800229

Reference yield: 37.0%

: C₂₆H₃₂O₈

: 1186018-78-9
3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

: C₂₆H₃₂O₈

Guidance literature:: With montmorillonite K-10; In dichloromethane; at 0 ℃; for 8h; Inert atmosphere;
DOI:10.1002/anie.201404499

Reference yield:

: 2'-hydroxy-2,4,4'-tri(methoxymethoxy)chalcone

: 1186018-78-9
3-(2,4-bis(methoxymethoxy)phenyl)-1-(2-hydroxy-4-(methoxymethoxy)-5-(3-methylbut-2-en-1-yl)phenyl)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 24 h / Reflux; Inert atmosphere

2: montmorillonite K-10 / dichloromethane / 8 h / 0 °C / Inert atmosphere

With potassium carbonate; In dichloromethane; acetone;
DOI:10.1002/anie.201404499