(3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol

Base Information

• Chemical Name: (3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol
• CAS No.: 120143-61-5
• Molecular Formula: C₃₀H₃₄O₆
• Molecular Weight: 490.596

Synonyms:(3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol

Chemical Property of (3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol

Chemical Property:

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Technology Process of (3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol

There total 49 articles about (3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(1R,4S)-4,7,7-Trimethyl-3-oxo-2-oxa-bicyclo[2.2.1]heptane-1-carboxylic acid (3aR,4S,5R,6S,7S,7aR)-4,6,7-tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-yl ester (114218-18-7,120143-58-0,120143-99-9,125474-18-2,125474-24-0,141040-42-8) → (3aR,4R,5R,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol (120143-61-5)

Guidance literature:

With potassium hydroxide; In methanol;

DOI:10.1016/S0040-4039(00)80720-0

Reference yield: 92.0%

(+/-)-2,5,6-tri-O-benzyl-myo-inositol (98906-30-0,104873-76-9,111466-07-0,114297-88-0,114297-91-5,114419-08-8,115184-71-9,115509-75-6,115509-76-7,118354-54-4,118354-55-5,128163-34-8,129706-80-5,136521-84-1,149713-88-2,149713-95-1) + 2,2-dimethoxy-propane (77-76-9) → (+/-)-1,6-O-isopropylidene-2,4,5-tri-O-benzyl-myo-inositol (111446-91-4,114297-90-4,114297-93-7,120143-57-9,120143-61-5,120143-62-6,125474-19-3,149713-81-5,149713-82-6)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; at 25 ℃; for 3.5h;

DOI:10.1016/0008-6215(92)85039-3

Reference yield: 82.0%

(±)-2,3,6-tri-O-benzyl-myo-inositol (98906-30-0,104873-76-9,111466-07-0,114297-88-0,114297-91-5,114419-08-8,115184-71-9,115509-75-6,115509-76-7,118354-54-4,118354-55-5,128163-34-8,129706-80-5,136521-84-1,149713-88-2,149713-95-1) + 2,2-dimethoxy-propane (77-76-9) → (+/-)-1,2,4-tri-O-benzyl-5,6-O-isopropylidene-myo-inositol (111446-91-4,114297-90-4,114297-93-7,120143-57-9,120143-61-5,120143-62-6,125474-19-3,149713-81-5,149713-82-6)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 2h;

upstream raw materials:

benzyl bromide

(±)-1,2-O-isopropylidene-3,6-di-O-benzyl-myo-inositol

(+/-)-1,2-O-isopropylidene-myo-inositol

(±)-1,2:5,6-di-O-isopropylidene-myo-inositol

Downstream raw materials:

L-myo-inositol 1,3,4-trisphosphate hexasodium salt

(-)-1L-2,5,6-tri-O-benzyl-1,3,4-tris(dibenzylphospho)-myo-inositol

(3aR,4R,5S,6R,7S,7aR)-4,6,7-Tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-ol

(1R,4S)-4,7,7-Trimethyl-3-oxo-2-oxa-bicyclo[2.2.1]heptane-1-carboxylic acid (3aR,4S,5R,6S,7S,7aR)-4,6,7-tris-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-5-yl ester

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