1,4-{C₃F₇OCF(CF₃)C(O)}2-C₆F₄

Base Information

• Chemical Name: 1,4-{C₃F₇OCF(CF₃)C(O)}2-C₆F₄
• CAS No.: 70815-67-7
• Molecular Formula: C₁₈F₂₆O₄
• Molecular Weight: 774.154

Synonyms:1,4-{C₃F₇OCF(CF₃)C(O)}2-C₆F₄

Chemical Property of 1,4-{C₃F₇OCF(CF₃)C(O)}2-C₆F₄

Chemical Property:

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Technology Process of 1,4-{C₃F₇OCF(CF₃)C(O)}2-C₆F₄

There total 3 articles about 1,4-{C₃F₇OCF(CF₃)C(O)}2-C₆F₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

perfluoro(2-propoxypropionyl) fluoride (2062-98-8,125037-08-3,75566-60-8) + 4-bromotetrafluorophenylmagnesium bromide (31103-33-0) → bromobenzene (108-86-1,52753-63-6) + 1-bromo-2,3,5,6-tetrafluorobenzene (1559-88-2) + 4-Br-C6F4C(O)CF(CF3)OC3F7 (70628-03-4) + 1,4-{C3F7OCF(CF3)C(O)}2-C6F4 (70815-67-7)

Guidance literature:

In diethyl ether; -20°C, 12 d;

DOI:10.1016/S0022-1139(00)82083-7

Reference yield:

perfluoro(2-propoxypropionyl) fluoride (2062-98-8,125037-08-3,75566-60-8) + 4-bromotetrafluorophenylmagnesium bromide (31103-33-0) → 1,4-dibromotetrafluorobenzene (344-03-6) + 1,4-{C3F7OCF(CF3)C(O)}2-C6F4 (70815-67-7)

Guidance literature:

In tetrahydrofuran; 0°C, 2 h , ratio of products = 1:1;

DOI:10.1016/S0022-1139(00)82083-7

Reference yield:

→ 1,4-{C3F7OCF(CF3)C(O)}2-C6F4 (70815-67-7)

Guidance literature:

aus Et-MgBr, 1) p-BrC6F4Br, 2) C3F7-O-CF(CF3)-C(O)-F;

DOI:10.1016/S0022-1139(00)82083-7

upstream raw materials:

perfluoro(2-propoxypropionyl) fluoride

4-bromotetrafluorophenylmagnesium bromide

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