7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

Base Information

Chemical Name:7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile
CAS No.:109912-35-8
Molecular Formula:C₂₃H₃₂N₄O
Molecular Weight:380.533
Hs Code.:

Synonyms:7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

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Chemical Property of 7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

Chemical Property:

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Technology Process of 7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

There total 4 articles about 7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20965-27-9
7-bromo-heptanonitrile

: 104499-47-0
N-Desmethylpyrilamine

: 109912-35-8
7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.1016/0223-5234(87)90002-X

Reference yield:

: 109-04-6
2-bromo-pyridine

: 109912-35-8
7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / pyridine / 5 h / Heating

2: 71 percent / sodium hydride / dimethylsulfoxide / 1.) below 40 deg C, 20 min, 2.) 22 deg C, 45 min

3: 91 percent / acetic anhydride / diethyl ether / 16 h / 22 °C

4: 95 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

5: potassium carbonate / dimethylformamide / 2 h / 100 °C

With lithium aluminium tetrahydride; acetic anhydride; sodium hydride; potassium carbonate; In tetrahydrofuran; pyridine; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(87)90002-X

Reference yield:

: 74764-17-3
2-[(pyridin-2-yl)amino]ethylamine

: 109912-35-8
7-({2-[(4-Methoxy-benzyl)-pyridin-2-yl-amino]-ethyl}-methyl-amino)-heptanenitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / sodium hydride / dimethylsulfoxide / 1.) below 40 deg C, 20 min, 2.) 22 deg C, 45 min

2: 91 percent / acetic anhydride / diethyl ether / 16 h / 22 °C

3: 95 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

4: potassium carbonate / dimethylformamide / 2 h / 100 °C

With lithium aluminium tetrahydride; acetic anhydride; sodium hydride; potassium carbonate; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(87)90002-X