(Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime

Base Information

• Chemical Name: (Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime
• CAS No.: 201206-10-2
• Molecular Formula: C₈H₆BrCl₂NO
• Molecular Weight: 282.952
• Mol file: 201206-10-2.mol

Synonyms:(Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime

Chemical Property of (Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime

There total 2 articles about (Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(4-bromo-phenyl)-2,2-dichloro-ethanone (7716-86-1) → (Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime (201206-10-2)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 48h; Ambient temperature;

DOI:10.1039/a704408i

Reference yield:

para-bromoacetophenone (99-90-1) → (Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime (201206-10-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Cl₂ / acetic acid / 40 - 59 °C

2: 85 percent / NH₂OH*HCl / ethanol / 48 h / Ambient temperature

With hydroxylamine hydrochloride; chlorine; In ethanol; acetic acid;

DOI:10.1039/a704408i

Reference yield: 97.0%

(Z)-1-(4-Bromophenyl)-2,2-dichloroethanone oxime (201206-10-2) → 3-(4-Bromo-phenyl)-4-chloro-[1,2,5]thiadiazole

Guidance literature:

With tetrasulphur tetranitride; In 1,4-dioxane; for 6h; Heating;

DOI:10.1039/a704408i

upstream raw materials:

1-(4-bromo-phenyl)-2,2-dichloro-ethanone

para-bromoacetophenone